电刷镀-电接触强化复合工艺制备厚镀层研究

    Study on Thick Coating Prepared by Composite Process of Brush Plating and Electric Contact Strengthening

    • 摘要: 利用电刷镀-电接触强化复合工艺,在球墨铸铁表面制备了1.6 mm镍镀层。利用超景深显微镜、显微硬度测试仪分析镀层强化前后的组织与性能,并按照QB/T3821-1999对镀层进行锉刀试验。结果表明,随着镀层厚度的增加,裂纹、孔洞等缺陷增多。镀层的整体组织特征可大致分3个区域,靠近基体的“裂纹区”、中部的“孔隙区”、表层的“疏松区”。在电刷镀的晶粒沉积过程中,缺陷的形成与晶粒团之间的碰撞与合并有关。电接触强化后,镀层组织致密,缺陷被压合,区域特征基本消失,仅镀层边缘处仍存在少量缺陷,硬度由473.50 HV提升到540.32 HV。这主要由于电接触强化热压耦合的作用,缺陷和界面处接触电阻最大,受热集中,且界面缝隙处与镀层缺陷处的流动阻力最小,缺陷易得到填充。锉刀试验后,发现强化前镀层剥落,而强化后镀层未剥落,表明电接触强化提高了镀层与基体的结合力。进一步分析界面处,发现镀层与基体之间出现局部互熔、搭桥及镶嵌的现象。

       

      Abstract: 1.6 mm nickel coating was prepared on the surface of nodular cast iron by composite process of brush plating and electric contact strengthening. The microstructure of raw coating and strengthened coating was analyzed by ultra depth of field microscope and hardness tester, and the coatings were tested by file according to QB/T3821-1999. The results show that the defects such as cracks and holes increase with growing of coating. The overall microstructure characteristics of the raw coating can be roughly divided into three areas, such as the "crack area" near the substrate, the "pore area" in the middle and the "loose area" in the surface. In the process of grain deposition of brush plating, the formation of defects is related to the collision and mergence between grain clusters. After strengthening, the regional characteristics basically disappear, the gaps are pressed, and few defects exist at the outer edge of coating, with coating’s hardness increasing from 473.50 HV to 540.32HV. This is mainly due to the coupling effect of heat and press of electric contact strengthening. The resistance between defect and interface is highest with heating concentrated, and the drag forces at the interface or gaps are weakest, so the defects there are filled more easily. After file test, it is found that the coating is peeled off before strengthening, but not after strengthening,indicating that the electrical contact strengthening could improve the adhesion between the coating and substrate. The further analysis of the interface shows that there are local mutual fusion, bridging and inlay between the coating and the matrix.

       

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