退火态钨钾合金的微结构演化及力学性能研究

    Study on Microstructure Evolution and Mechanical Properties of Annealed W-K Alloy

    • 摘要: 钨基材料因其高熔点、相对优异的高温性能被广泛应用于核聚变及搅拌摩擦焊接领域。以钨钾合金为对象,研究退火态钨钾合金的微观组织演变及相应力学性能。结果表明:原始态钨钾合金的平均晶粒尺寸、平均硬度分别为2.08 μm、4.38 GPa,800℃抗拉强度423 MPa、断裂伸长率50%。锻态钨钾合金的再结晶温度在1425~1435℃。当退火温度低于1425℃,钨钾合金以回复为主。1425℃退火态样品平均晶粒尺寸为2.23 μm,较原始态的增大22%,平均硬度下降4%至4.21 GPa,800℃抗拉强度为393 MPa,断裂伸长率为34%。当退火温度达到1500℃,材料完成再结晶,晶粒出现明显粗化,平均晶粒尺寸为178.17 μm,是原始态样品平均晶粒尺寸的85倍,平均硬度为3.60 GPa,较原始态下降18%,800℃抗拉强度仅为208 MPa,断裂伸长率为44%。

       

      Abstract: Tungsten-based materials have good prospects as candidate materials for nuclear fusion devices and friction stir welding tools due to their high melting point and relatively excellent high-temperature mechanical properties.The microstructure and corresponding mechanical properties of as-received and annealed W-K alloy were investigated.The results show that the average grain size of as-received W-K alloy is 2.08 μm, with the average hardness values of 4.38 GPa.When the ambient temperature is up to 800 ℃, the ultimate tensile strength of as-forged W-K alloy is 423 MPa, accompanied with fracture elongation being 50%.The recrystallization temperature of the forged W-K alloy ranges from 1425 ℃to 1435 ℃.Recovery dominates inside the W-K material as the annealing temperature is lower than 1425 ℃.Compared with corresponding data of as-received samples, the average grain size increases by 22% to 2.23 μm while the average hardness decreases by 4%to 4.21 GPa with the tensile properties being characterized by the ultimate tensile strength reduces to 393MPa and fracture elongation descends to 34%as W-K alloy is annealed at 1425℃.When the annealing temperature is up to 1500℃, the recrystallization is finished along with grain coarsening.The average grain size is 178.17 μm, which is 84 times bigger than average grain size of original samples, meanwhile the average hardness drops by 18% to 3.60 GPa compared with as-forged samples.When the ambient temperature rises up to 800 ℃, the ultimate tensile strength of the W-K alloy annealed at 1500 ℃decreases dramatically to 208 MPa, and the fracture elongation is 44%.

       

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