层厚比对Al2O3-ZrB2/Al2O3-TiCN层状陶瓷微观组织和力学性能的影响

    Effects of Layer Thickness Ratio on Microstructure and Mechanical Properties of Al2O3-ZrB2/Al2O3-TiCN Laminated Ceramics

    • 摘要: 以Al2O3为各层的基体相,Y2O3为各层的烧结助剂,Zr B2、Ti C0.7N0.3分别为AZ层和AT层的添加相,利用粉末旋转铺层法和真空热压烧结技术,在1650℃下制备了具有不同层厚比的Al2O3-Zr B2/Al2O3-Ti CN层状陶瓷,研究了层厚比对其微观组织和力学性能的影响。结果表明:随着层厚比的增大,层状陶瓷的相对密度、维氏硬度、抗弯强度均呈现先增大后减小的趋势,而其断裂韧性逐渐增大。层厚比为4∶1时,材料的致密度较高,晶粒相对较小且分布均匀,获得了较好的综合力学性能,其分别为表层维氏硬度(19.28±0.25)GPa、抗弯强度(637.68±20)MPa、表层断裂韧性(7.81±0.35) MPa·m1/2

       

      Abstract: Al2O3-ZrB2/Al2O3-TiCN layered ceramics with different layer thickness ratios were prepared at 1650 ℃ by powder rotating layer method and vacuum hot pressing sintering technology with Al2O3 as the matrix phase of each layer, Y2O3 as the sintering aid of each layer, ZrB2 and TiC0.7N0.3as the additive phases of AZ layer and AT layer, respectively. The effects of layer thickness ratio on the microstructure and mechanical properties were studied. The results show that with the increase of layer thickness ratio, the relative density, Vickers hardness and bending strength of laminated ceramics increase first and then decrease, while the fracture toughness increases gradually. When the layer thickness ratio is 4∶1, the relative density of the material is higher, the grains are relatively small and uniformly distributed, and good comprehensive mechanical properties are obtained, which are surface Vickers hardness of(19.28±0.25) GPa, bending strength of(637.68±20) MPa, surface fracture toughness of(7.81±0.35) MPa·m1/2, respectively.

       

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