不同回流状态下选区激光熔化316L成型件组织和性能对比分析

    Comparative Analysis on Microstructure and Properties of 316L Formed Parts by Selective Laser Melting under Different Reflux Conditions

    • 摘要: 采用选区激光熔化设备在有无回流状态下进行打印。利用扫描电镜(SEM)、X射线衍射(XRD)对打印成型件的微观组织、物相、断口进行研究。结果表明:两组成型件的物相均为奥氏体相,微观组织呈胞状晶,受快速非平衡凝固与马兰戈尼对流的影响,胞状晶的结晶位向表现出各向异性。无回流状态的成型件表面整洁;有回流状态的成型件表面有很多微米级别的颗粒,而且熔道出现了部分中断现象,经过深度腐蚀之后,内部可以观测到孔洞、未熔化的粉末。无回流状态的拉伸断口中存在大量等轴韧窝;有回流的拉伸断口韧窝呈现“倭瓜”状,同时在断口中可观察到很多的孔洞。与无回流试样相比,在回流状态下试样的抗拉强度减少了51.98 MPa,伸长率减少了7.39%。在回流情况下成型件内部的夹渣、未熔颗粒、孔洞减少了试样承载面积,造成了应力集中,降低了成型件的力学性能。

       

      Abstract: The samples were prepared by selective laser melting equipment in the presence and absence of reflux. Then, the microstructure, phase and fracture of the printed parts were analyzed by scanning electron microscopy (SEM) and X-ray diffraction (XRD).The results show that the phase of the two formed parts is austenite phase, and the microstructure presents cellular crystals.Under the influence of rapid non-equilibrium solidification and Marangoni convection, the crystal orientation of the cellular crystal exhibits anisotropy. The surface of the part prepared in the absence of reflux is smooth and neat; there are many micron-level particles on the surface of the part prepared in the reflux state, and the melt channel is partially interrupted. After the deep corrosion, holes and unmelted powder can be observed inside. There are a large number of equiaxed dimples in the fracture of the part prepared without reflux. The dimples in the fracture of the part prepared in the reflux state show the shape of “pumpkin”, and many holes can be observed in the fracture. By comparing those of the sample without reflux, the tensile strength of the sample in the presence of reflux is reduced by 51.98 MPa and the elongation is reduced by 7.39%. The internal defects such as slag inclusion, unmelted particles and holes in the part prepared in the presence of reflux reduce the bearing area of the sample, which causes stress concentration and reduces the mechanical properties of the part.

       

    /

    返回文章
    返回