稀土Gd含量对Mg-xGd-3Y-(1Zn)-0.5Zr合金显微组织和力学性能的影响

    Effect of Gd Content on Microstructure and Mechanical Properties of Mg-xGd-3Y-(1Zn)-0.5Zr Alloys

    • 摘要: 采用高通量真空熔炼炉制备Mg-xGd-3Y-(1Zn)-0.5Zr合金。利用光学显微镜(OM)、扫描电子显微镜(SEM)、能谱分析仪(EDS)、X射线衍射仪(XRD)、场发射扫描电镜(TEM)和MTS液压伺服试验机等测试设备,研究不同含量的Gd对铸态合金显微组织和力学性能的影响。结果表明:铸态合金组织由α-Mg基体、Mg5(Gd,Y)相和层片状18R-LPSO相组成。且随着Gd含量的增加,Mg5(Gd,Y)相和LPSO相体积分数逐渐增加,晶粒尺寸呈细化趋势,抗拉强度逐渐增强。Gd含量为10wt%的铸态合金表现出最佳的拉伸性能,其室温抗拉强度和屈服强度分别为271、196 MPa。

       

      Abstract: Mg-xGd-3Y-(1Zn)-0.5Zr alloys were prepared by high flux vacuum melting furnace. Optical microscope (OM), scanning electron microscope (SEM), energy dispersive spectrometer (EDS), X-ray diffractometer (XRD), field emission trams mission electron microscope (TEM) and MTS hydraulic servo testing machine were used to study the effects of different Gd contents on the microstructure and mechanical properties of the as-cast alloys. The results show that the microstructure of the as-cast alloys is composed of α-Mg matrix, Mg5(Gd, Y) phase and lamellar 18R-LPSO phase. With the increase of Gd content, the volume fraction of Mg5(Gd, Y) phase and LPSO phase gradually increase, the grain size shows a trend of refinement, and the tensile strength gradually increases. The as-cast alloy with the Gd content of 10wt% has the best tensile properties, and its tensile strength and yield strength at room temperature are 271 MPa and 196 MPa, respectively.

       

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