VW94稀土镁合金放电等离子扩散连接工艺研究

    Study on Spark Plasma Diffusion Bonding Process of VW94 Rare Earth Magnesium Alloy

    • 摘要: 稀土镁合金作为优质轻量化金属材料在航空航天领域具有较好的应用前景。对不添加中间层和添加Cu、Ag、Ni中间层后的VW94稀土镁合金采用放电等离子扩散连接工艺(spark plasma diffusion bonding,SPDB),在480℃-2 MPa-120 min的工艺参数下,进行扩散连接试验,分析了扩散接头的微观组织和力学性能。结果表明:在不添加金属中间层的条件下,VW94稀土镁合金可以实现高质量扩散连接,界面剪切强度109 MPa;Cu、Ag中间层分别可与稀土镁合金形成良好扩散接头,Cu原子主要扩散到LPSO相中形成Mg12(Gd,Y)1(Cu,Zn)1相,Ag原子则是会扩散溶入α-Mg基体中形成镁基固溶体Mg(ss,Ag),Zn、Zr原子会在接合面附近聚集,接合界面处剪切强度依次为106、109 MPa,分别达母材剪切强度的82.8%和85.2%;在此温度下,Ni原子基本没有发生扩散,接合界面剪切强度仅有16 MPa,仅达母材剪切强度的12.5%。

       

      Abstract: As a high-quality lightweight metal material, rare earth magnesium alloy has a good application prospect in the aerospace field. The spark plasma diffusion bonding(SPDB) process was used to join VW94 rare earth magnesium alloy without interlayer and with Cu, Ag and Ni interlayer. The diffusion bonding experiment was carried out under the process parameters of 480 ℃ -2 MPa-120 min. The microstructure and mechanical properties of the diffusion joint were analyzed.The results show that VW94 rare earth magnesium alloy can achieve high quality diffusion bonding without adding metal interlayer, and the interfacial shear strength is 109 MPa. The Cu and Ag interlayers can form good diffusion joints with rare earth magnesium alloy, respectively. Cu atoms mainly diffuse into the LPSO phase to form Mg12(Gd, Y)1(Cu, Zn)1 phase, and Ag atoms diffuse into the α-Mg matrix to form Mg-based solid solution Mg(ss, Ag). Zn and Zr atoms will gather near the joint surface. The shear strength of the joint interface is 106 MPa and 109 MPa, respectively, reaching 82.8% and 85.2% of the shear strength of the base material. At this temperature, Ni atoms basically do not diffuse, and the shear strength of the bonding interface is only 16 MPa, which was only 12.5% of the shear strength of the base metal.

       

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