应变速率对热挤压FGH96粉末高温合金微观组织的影响

    Effect of Strain Rate on Microstructure of Hot Extruded FGH96 Powder Metallurgy Superalloy

    • 摘要: 为研究应变速率对热挤压FGH96粉末高温合金过固溶处理后组织均匀性的影响,通过热模拟压缩和双锥试样等温压缩试验,并结合等温压缩试验有限元模拟,对比分析了不同应变速率下合金过固溶态晶粒组织的演变特征。研究发现,热模拟压缩试样经1070℃变形及1150℃过固溶后,均呈现粗细晶混合组织,且组织非均匀性随应变速率增大而显著增强,高应变速率下细小晶粒(<5 μm)与粗大晶粒(>45 μm)比例同时增加,晶粒尺寸分化加剧;低应变速率下晶粒分布则相对均匀。双锥试样在变截面顶角区域观察到明显的异常晶粒长大,尤其在0.1 mm/s低压下速率时最为严重,最大晶粒尺寸达587 μm。有限元模拟揭示,该异常长大并非由温升主导,而是归因于压缩后期顶角处应变速率的急剧升高,导致变形储能集中,进而在后续过固溶过程中引发不均匀长大。上述结果表明,应变速率是调控该类合金过固溶组织均匀性的关键工艺参数之一,为优化等温锻造工艺提供了直接依据。

       

      Abstract: To investigate the effect of strain rate on the microstructural homogeneity of hot extruded FGH96 powder metallurgy superalloy after supersolution treatment, thermal compression tests and double-cone isothermal compression experiments were conducted, combined with finite element simulations of isothermal compression experiments, the evolution characteristics of grain structures of the alloy in supersolution treated state under different strain rates were comparatively analyzed. The results show that the thermally compressed specimens deformed at 1070 ℃ and subsequently subjected to supersolution treatment at 1150 ℃ exhibit a mixed coarse-fine grain structure, and the microstructural heterogeneity increases significantly with the increase of the strain rate. At high strain rates, the proportions of both fine grains(<5 μm) and coarse grains(>45 μm) increase simultaneously, leading to intensified grain size differentiation, whereas a relatively uniform grain size distribution is obtained at low strain rates. For the double-cone specimens, pronounced abnormal grain growth is observed in the variable cross-section apex region, particularly under the low compression rate of 0.1 mm/s, the maximum grain size reaches 587 μm. Finite element simulations reveal that this abnormal grain growth is not primarily induced by temperature rise, but is attributed to the sharp increase in strain rate at the apex region during the later stage of compression. The localized concentration of deformation energy subsequently promotes heterogeneous grain growth during the supersolution treatment. These findings demonstrate that the strain rate is a critical process parameter for controlling the microstructural homogeneity of FGH96 powder metallurgy superalloy after supersolution treatment, providing direct guidance for the optimization of isothermal forging process.

       

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